XRF laboratóriumi mérés

Data provider

Budapest University of Technology and Economics, Department of Applied Biotechnology and Food Science, Environmental Microbiology and Biotechnology Group

Organisation/Data provider's nameBudapest University of Technology and Economics, Department of Applied Biotechnology and Food Science, Environmental Microbiology and Biotechnology Group
Name of contact
Dr. Molnár Mónika, Dr. Feigl Viktória
Contact details
Telephone/fax
+36-1-4632347
E-mail
mmolnar@mail.bme.hu
vfeigl@mail.bme.hu
Website
http://envirotox.hu
Compulsory sheet
Method Hungarian nameXRF laboratóriumi mérés
Method name
Laboratory use of the mobile XRF equipment
Stage of development
after application
Patent number
US EPA METHOD 6200
Contaminants
Chemical substance group|Typically treated chemical substance
  • Metals, semi-metals and their compounds
Feasibility of the method
Method type
measurement/analytical method
Place of application
In laboratory
Application areas of the method
Contaminant characterisationin in environmental element/phase/sample
Application possiblities of the method
Environmental monitoring
Screening of contaminated environment
Preliminary assessment of contaminated environment
Detailed assessment of contaminated environment
Technology monitoring
Environmental element/phase the method may be applied to
Unsaturated (whole) soil
Other non-environmental samples the method can be applied to
pl. ötvözetek, műanyagok
Implementation conditions
Instrument/equipment needed to perform the measurement
hordozható XRF készülék
Other necessary equipment/tools
dörzsmozsár a minta homogenizáláshoz, porításhoz, számítógép
Reagents/materials for the test
mintatartó vagy műanyag zacskó
How many samples are needed
minimum 20g
Data processing level
data input in PC, data evaluation by excel or other software
Necessary qualification
secondary education (chemical technician, chemical worker, laboratory assistant)
Type of laboratory
general analytical laboratory
Implementation costs
Purchase price of the equipment
20.000 - 40.000 Euro
Total cost/measurement
20 - 40 Euro
Innovation, main features
Brief concise description explaining the innovation

A hordozható XRF készülék jól használható talajok fémtartalmának meghatározásra, alkalmazása időt és költséget takarít meg a hagyományos analitikai vizsgálatokkal szemben.

Typical (recommended) application of the method

talajminták fémtartalmának meghatározására, de alkalmazzák ötvözetek, műanyagok, egyéb szilárd fázisú minták fémtartalmának meghatározására

Detailed Protocol

A talajmintákat a laboratóriumban homogenizáljuk, szárítjuk, porítjuk, majd zárható műanyag zacskóban vagy mintatartóba helyezve mérjük. A műszert bekapcsolás után, minden esetben kalibráljuk. A mintákat azonos ideig mérjük, ezzel kiküszöbölve a különböző időtartamú mérések által okozott hibát. A mérések optimális hossza 60-120 másodperc.

SWOT (evalaution based on scores)
Costs
4-low
Time requirement
4-low
Workload requirement
4-low
Equipment, apparata requirement
3-medium
Qualified labour
3-medium
Environmental risk and workplace risks
5-very low
Environmental reality
4-good
Adequate accuracy
4-good
Reproducibility
4-good
Cost efficiency
5-excellent
Feasibility
4-good
Availability
3-average
Well known
3-average
SWOT (evaluation in words)
Strengths

gyors, olcsó mérés, megfelelő pontosság, egyszeri beruházás után viszonylag alacsony egy mérésére jutó költség,

Weaknesses

a műszeres analitikai méréshez képest, nagyobb szórás, kisebb pontosság

Possibilities

ötvözetek, műanyagok fémtartalmának mérése

Other information, references
Webpage references and DEMO reports

www.niton.com, www,cason.hu
US EPA METHOD 6200

Publications

Tolner, M.; Nagy, G., Vaszita, E. and Gruiz, K.: In situ delineation of point sources and high resolution mapping of polluted sites by field-portable X-ray fluorescence measuring device. GREEN5 Conference, 1-4 July 2008

Kalniczy, D. J. and Singhvi, R.: Field portable XRF analysis of environmental samples. In: Journal of Hazardous Materials 83 pp. 93-122, Published by Elsevier Science B. V. 2001

Sarkadi, A.: In situ metal analysis by portable XRF device. MOKKA Conference, 15 June 2007, Budapest, Hungary

Completed applications
Location of the application, country
Magyarország
Location of the application, town and/or region
Gyöngyösoroszi
Environmental element the method was applied to
Environmental monitoring
Screening of contaminated environment
Preliminary assessment of contaminated environment
Detailed assessment of contaminated environment
Monitoring of contaminated environment
Environmental scenario the method was applied to
Terrestial habitat: polluted soil
Environmental element/phase the method was applied to
Unsaturated (whole) soil
Contaminant the method was applied to
Metals, semi-metals and their compounds
Adatlap tulajdonságai
Datasheet id (original)
33
Creator
Gruiz Katalin
Status
Verified
Adatlap típusaPhysico-chemical assessment methods
Létrehozás
Módosítás