Univerzális analitikai rendszer AOX, EOX, POX és AOS kulometriás meghatározására

Budapest University of Technology and Economics, Department of Applied Biotechnology and Food Science, Environmental Microbiology and Biotechnology Group

Organisation/Data provider's nameBudapest University of Technology and Economics, Department of Applied Biotechnology and Food Science, Environmental Microbiology and Biotechnology Group
Name of contact
Dr. Molnár Mónika, Dr. Feigl Viktória
Telephone/fax
+36-1-4632347
Method Hungarian nameUniverzális analitikai rendszer AOX, EOX, POX és AOS kulometriás meghatározására
Method name
Universal analytical system for determination of AOX, EOX, POX and TOX
Stage of development
after application
Chemical substance group|Typically treated chemical substance
  • Halogenated aliphatic organic compounds
Chemical substance group|Typically treated chemical substance
  • Halogenated aromatic organic compounds
Detection limit
0.1 µg
Reproducibility (%)
1.00
Selectivity
non-selective
Method type
measurement/analytical method
Place of application
In laboratory
Application areas of the method
Contaminant characterisationin in environmental element/phase/sample
Characterisation of water ecosystem
Application possiblities of the method
Screening of contaminated environment
Monitoring of contaminated environment
Environmental element/phase the method may be applied to
Saturated soil
Unsaturated (whole) soil
Subsurface water
Surface water
Surface water sediment
Leachate
Instrument/equipment needed to perform the measurement
Behr Cl10 készülék
Other necessary equipment/tools
mérleg
Standard materials for the test
abszolút módszer, kalibrálás nem szükséges
Reagents/materials for the test
gázok (Ar, O2)
How many samples are needed
10-100 ml vagy 5 g
Data processing level
data collection, recording, evaluation by software
Necessary qualification
secondary education (chemical technician, chemical worker, laboratory assistant)
Type of laboratory
no need for laboratory, in situ or on site measurement is possible
Purchase price of the equipment
20.000 - 40.000 Euro
Labour cost/measurement
0 - 2 Euro
Total cost/measurement
4 - 8 Euro
Brief concise description explaining the innovation

Újdonság a programozható infravörös kályha extrém gyors felfűtéssel és lehűtéssel (A Behr Labor fejlesztése). AOX adszorpció aktív szén oszlopon, EOX extrakció, befecskendezés automata mintaadagolóval, POX kihajtás termosztált mintából. A minták az égető kemencébe jutnak, majd a felszabaduló halogénsavakat kulometriásan titrálja a készülék.

Detailed Protocol

A minta bemérésén kívül a készülék mindent automatikusan elvégez.

Costs
3-medium
Time requirement
4-low
Workload requirement
4-low
Equipment, apparata requirement
2-high
Qualified labour
3-medium
Environmental risk and workplace risks
4-low
Environmental reality
3-average
Adequate accuracy
4-good
Reproducibility
4-good
Feasibility
4-good
Availability
4-good
Well known
4-good
Strengths

gyors felfűtés és lehűtés (1 AOX mérés 5 perc), széles mérési tartomány (0,1-300ug Cl-), pontos potenciálmeghatározás, 5 mikroV felbontás

Weaknesses

drága készülék

Webpage references and DEMO reports
Publications

M. Hahn, ....: A new measuring device for the rapid coulometric determination of adsorbable organic halogen compounds. Fresenius J. Anal. Chem. 340, 22-26 (1991)

Location of the application, country
Magyarország
Location of the application, town and/or region
Budapest
Application areas
Contaminant characterisationin in environmental element/phase/sample
General characterisation of surface water
Contaminant the method was applied to
Halogenated aliphatic organic compounds
Datasheet id (original)
781
Creator
Fenyvesi Éva
Status
Verified
Adatlap típusaPhysico-chemical assessment methods
Létrehozás
Módosítás